Handbook of analytical instruments / Dr R S Khandpur.

Format:

Book

Author/Creator:

Khandpur, Raghbir Singh, 1942- author.

Language:

English

Subjects (All):

Chemical apparatus--Handbooks, manuals, etc.

Chemical apparatus.

Physical instruments--Handbooks, manuals, etc.

Physical instruments.

Analytical chemistry--Instruments.

Analytical chemistry.

Physical Description:

1 online resource (xxii, 770 pages) : illustrations, figs., tables.

Edition:

2nd edition.

Place of Publication:

New York, N.Y. : McGraw-Hill Education LLC., c2006.

Contents:

A. Preface to the second edition

B. Acknowledgements

C. Preface to the first edition

1. Fundamentals of analytical instruments

Elements of an analytical instrument

Sensors and transducers

Signal conditioning in analytical instruments

Read-out (display) systems

Intelligent analytical instrumentation systems

Pc-based analytical instruments

Performance requirements of analytical instruments

Instrument calibration techniques

Validation

2. Colorimeters and spectrophotometers (visible?ultraviolet)

Electromagnetic radiation

Laws relating to absorption of radiation

Absorption instruments

Ultraviolet and visible absorption spectroscopy (uv?vis)

Colorimeters/photometers

Spectrophotometers

Sources of error in spectrophotometric measurements

Calibration

3. Infrared spectrophotometers

Infrared spectroscopy

Basic components of infrared spectrophotometers

Types of infrared spectrophotometers

Sample handling techniques

Fourier transform infrared spectroscopy (ftir)

Attenuated total reflectance (atr) technique

4. Flame photometers

Principle of flame photometry

Constructional details of flame photometers

Types of flame photometers

Clinical flame photometers

Accessories for flame photometer

Expression of concentration

Interferences in flame photometry

Procedure for determinations

5. Atomic absorption spectrophotometers

Atomic absorption spectroscopy

Atomic absorption instrumentation

Sources of interferences

Meter scale

6. Fluorimeters and phosphorimeters

Fluorescence spectroscopy

Principle of fluorescence

Measurement of fluorescence

Spectrofluorimeters

z#REF!Microprocessor-based spectrofluorometer

Measurement of phosphorescence

7. Raman spectrometer

The raman effect

Raman spectrometer

Pc-based raman spectrometer

Infrared and raman microspectrometry

8. Photoacoustic and photothermal spectrometers

Photoacoustic spectroscopy

Photothermal spectroscopy

9. Mass spectrometer

Basic mass spectrometer

Principle of operation

Types of mass spectrometers

Components of a mass spectrometer

Inductively coupled plasma?mass spectrometer

Trapped ion mass analyzers

Ion cyclotron resonance (icr) mass spectrometery

Quadrupole ion trap mass spectrometer

Resolution in mass spectrometry

Applications of mass spectrometry

Gas chromatograph?mass spectrometer (gc?ms)

Liquid chromatograph?mass spectrometer

Tandem mass spectrometry (ms/ms)

10. Nuclear magnetic resonance spectrometer

Nuclear magnetic resonance spectroscopy

Principle of nmr

Types of nmr spectrometers

Constructional details of nmr spectrometer

Varian t-60a nmr spectrometer

Sensitivity enhancement for analytical nmr spectroscopy

Fourier transform nmr spectroscopy

11. Electron spin resonance spectrometers

Electron spin resonance

Basic esr spectrometer

Detailed description of an esr spectrometer

12. Electron and ion spectrometers

Surface spectroscopic techniques

Electron spectroscopy

Instrumentation for electron spectroscopy

Ion spectroscopy

Scanning tunnelling microscopy

Atomic force microscopy.

13. Radiochemical instruments

Fundamentals of radiochemical methods

Radiation detectors

Liquid scintillation counters

Pulse?height analyzer

Gamma spectrometry

14. X-ray spectrometers

X-ray spectrum

Instrumentation for x-ray spectrometry

X-ray diffractometers

X-ray absorption meter

X-ray fluorescence spectrometry

Electron probe microanalyzer

15. Automated chemical analysis systems

Why automate?

Automated biochemical analysis system

Advanced versions of multiple analysis system

Flow injection analysis (fia) technique

Lab-on-chip technology for automated analysis

16. Gas chromatographs

Chromatography

Basic definitions

Gas chromatography

Basic parts of a gas chromatograph

Methods of measurement of peak areas

17. Liquid chromatographs

Liquid chromatography

Types of liquid chromatography

High pressure liquid chromatograph (hplc)

Amino-acid analyzers

18. Thermo-analytical instruments

Thermo-analytical methods

Thermogravimetric analysis (tga)

Differential thermal analysis (dta)

Differential scanning calorimetry

Simultaneous thermal analysis/mass spectrometer

19. Electrophoresis apparatus and densitometers

Electrophoresis

Electrophoresis techniques

Paper electrophoresis

Electrophoresis apparatus

Spectrodensitometers

Microprocessor-based densitometer

Capillary electrophoresis

Micro-electrophoresis

Steps in the electrophoresis procedure requiring quality control

Electrochemical cell

Potentiostats

Types of electrochemical methods

Potentiometers

Conductivity meters

Voltametry

Polarographs

Coulometers

Amperometers

Aquameters

Microcomputer-controlled electrochemical instrumentation

21. Ph meters and ion analyzers

What is ph ?

Principle of ph measurement

Electrodes for ph measurement

Ph meters

Selective ion electrodes

Ion analyzer

Chemically sensitive semiconductor devices

Biosensors

22. Blood gas analyzers

Acid base balance

Blood ph measurement

Measurement of blood pco_2

Blood po_2 measurement

A complete blood gas analyzer

23. Industrial gas analyzers

Types of gas analyzers

Paramagnetic oxygen analyzer

Magnetic wind instruments

The electrochemical methods

Infrared gas analyzers

Thermal conductivity analyzers

Analyzers based on gas density

Method based on ionization of gases

24. Environmental pollution monitoring instruments

Air pollution monitoring instruments

Carbon monoxide

Sulphur dioxide

Nitrogen oxides

Hydrocarbons

Ozone

Automated wet-chemical air analysis

Water pollution monitoring instruments

25. Electronic devices and circuits

Electronic components

Passive components

Semiconductor devices

Transistors

Integrated circuits

Operational amplifiers

Sources of noise in electronic circuits

Sources of noise in low?level measurements

Noise reduction techniques

26. Digital circuits

Digital circuits

Types of logic circuits

Logic families

Categories of ic's based on packing density

Typical digital integrated circuits

Semiconductor memories

Microprocessor

Microcontrollers

Data converters

Data acquisition systems for analytical instruments

27. Computer-based analytical instruments

Computers in analytical laboratories

Digital computer

Microcomputers

Components of a microcomputer

Computer software

Connecting laboratory instruments to computers

A. References.

Notes:

Includes bibliographical references and indexes.

Description based on cover image and table of contents, viewed on Jul. 16, 2015.

ISBN:

9780070604605

0070604606

9780071487467

0071487468

Access Restriction:

Restricted for use by site license.