High-resolution NMR techniques in organic chemistry / Timothy D. W. Claridge

Format:

Book

Author/Creator:

Claridge, Timothy D. W., author.

Language:

English

Subjects (All):

Nuclear magnetic resonance spectroscopy.

Organic compounds--Analysis.

Organic compounds.

Chemistry, Organic.

Physical Description:

1 online resource (x, 543 pages) : illustrations

Edition:

Third edition

Place of Publication:

Amsterdam, [Netherlands] : Elsevier, [2016]

Summary:

High-Resolution NMR Techniques in Organic Chemistry, Third Edition describes the most important NMR spectroscopy techniques for the structure elucidation of organic molecules and the investigation of their behaviour in solution. Appropriate for advanced undergraduate and graduate students, research chemists and NMR facility managers, this thorough revision covers practical aspects of NMR techniques and instrumentation, data collection, and spectrum interpretation. It describes all major classes of one- and two-dimensional NMR experiments including homonuclear and heteronuclear correlations, the nuclear Overhauser effect, diffusion measurements, and techniques for studying protein–ligand interactions. A trusted authority on this critical expertise, High-Resolution NMR Techniques in Organic Chemistry, Third Edition is an essential resource for every chemist and NMR spectroscopist.

Contents:

1. Introduction

2. Introducing High-Resolution NMR

3. Practical Aspects of High-Resolution NMR

4. One-Dimensional Techniques

5. Introducing Two-Dimensional and Pulsed Field Gradient NMR

6. Correlations Through the Chemical Bond I: Homonuclear Shift Correlation

7. Correlations Through the Chemical Bond II: Heteronuclear Shift Correlation

8. Separating Shifts and Couplings: J-Resolved and Pure Shift Spectroscopy

9. Correlations Through Space: The Nuclear Overhauser Effect

10. Diffusion NMR Spectroscopy

11. Protein

Ligand Screening by NMR

12. Experimental Methods

13. Structure Elucidation and Spectrum Assignment.

Notes:

Includes bibliographical references at the end of each chapters and index.

Description based on online resource; title from PDF title page (ebrary, viewed May 19, 2016).

ISBN:

9780080999937

008099993X

OCLC:

948173049