Solving problems with NMR spectroscopy / Atta-ur-Rahman and Muhammad Iqbal Choudhary.

Format:

Book

Author/Creator:

Rahman, Atta-ur-, 1942-

Contributor:

Choudhary, Muhammad Iqbal.

Language:

English

Subjects (All):

Nuclear magnetic resonance spectroscopy.

Nuclear spectroscopy.

Physical Description:

1 online resource

Edition:

Second edition

Place of Publication:

San Diego : Academic Press, c1996.

Language Note:

English

Summary:

Solving Problems with NMR Spectroscopy presents the basic principles and applications of NMR spectroscopy with only as much math as is necessary. It shows how to solve chemical structures with NMR by giving clear examples and solutions. This text will enable organic chemistry students to choose the most appropriate NMR techniques to solve specific structures. The problems to work and the discussion of their solutions and interpretations will help readers becomeproficient in the application of important, modern 1D and 2D NMR techniques to structural studies.Key Features* Pres

Contents:

Front Cover; Solving Problems with NMR Spectroscopy; Copyright Page; Contents; Foreword; Foreword; Preface; Chapter 1. The Basics of Modern NMR Spectroscopy; 1.1 WHAT IS NMR?; 1.2 INSTRUMENTATION; 1.3 CREATING NMR SIGNALS; SOLUTIONS TO PROBLEMS; REFERENCES; Chapter 2. Spin-Echo and Polarization Transfer; 2.1 SPIN-ECHO FORMATION IN HOMONUCLEAR AND HETERONUCLEAR SYSTEMS; 2.2 CROSS-POLARIZATION; 2.3 POLARIZATION TRANSFER IN REVERSE; SOLUTIONS TO PROBLEMS; REFERENCES; Chapter 3. The Second Dimension; 3.1 DATA ACQUISITION IN 2D NMR; 3.2 DATA PROCESSING IN 2D NMR; 3.3 PLOTFING OF 2D SPECTRA

SOLUTIONS TO PROBLEMSREFERENCES; Chapter 4. Nuclear Overhauser Effect; 4.1 nOe AND SELECTIVE POPULATION TRANSFER; 4.2 RELAXATION; 4.3 MECHANISM OF nOe; 4.4 FACTORS AFFECTING nOe; 4.5 SOME PRACTICAL HINTS; SOLUTIONS TO PROBLEMS; REFEREN CES; Chapter 5. Important 2D NMR Experiments; 5.1 HOMO- AND HETERONUCLEAR J-RESOLVED SPECTROSCOPY; 5.2 HOMONUCLEAR AND HETERONUCLEAR SHIFT- CORRELATION SPECTROSCOPY; 5.3 TWO-DIMENSIONAL NUCLEAR OVERHAUSER SPECTROSCOPY; 5.4 TWO-DIMENSIONAL CHEMICAL EXCHANGE SPECTROSCOPY

5.5 HOMONUCLEAR HARTMANN-HAHN SPECTROSCOPY (HOHAHA), OR TOTAL CORRELATION SPECTROSCOPY (TOCSY)5.6 ""INVERSE"" NMR SPECTROSCOPY; 5.7 INADEQUATE; SOLUTIONS TO PROBLEMS; REFERENCES; Chapter 6. The Third Dimension; 6.1 BASIC PHILOSOPHY; 6.2 TYPES AND POSITIONS OF PEAKS IN 3D SPECTRA; REFERENCES; Chapter 7. Recent Developments in NMR Spectroscopy; 7.1 SELECTIVE PULSES IN MODERN NMR SPECTROSCOPY; 7.2 ONE-DIMENSIONAL EXPERIMENTS USING SOFT PULSES; 7.3 HETERONUCLEAR SELECTIVE 1D NMR EXPERIMENTS; 7.4 TWO-DIMENSIONAL EXPERIMENTS USING SOFT PULSES; 7.5 SOFT EXCITATION IN TWO DIMENSIONS

7.6 THREE-DIMENSIONAL EXPERIMENTS USING SOFT PULSES7.7 FIELD GRADIENTS; REFERENCES; Chapter 8. Logical Protocols for Solving Complex Structural Problems; 8.1 3-HYDROXYLUPANINE (1); 8.2 (+)-BUXALONGIFOLAMIDINE (2); REFERENCES; GLOSSARY; Index

Notes:

Description based upon print version of record.

Includes bibliographical references and index.

ISBN:

1-281-05376-7

9786611053765

0-08-054149-6

OCLC:

476103589