Comprehensive guide for mesoporous materials. Volume 2 : analysis and functionalization / Mahmood Aliofkhazraei, editor.

Format:

Book

Contributor:

Aliofkhazraei, Mahmood, editor.

Series:

Materials science and technologies series.

Materials Science and Technologies

Language:

English

Subjects (All):

Mesoporous materials.

Mesoporous materials--Analysis.

Physical Description:

1 online resource (427 p.)

Place of Publication:

New York, New York : Nova Science Publishers, Inc., 2015.

Language Note:

English

Summary:

This is the second volume of the four volume set of the Comprehensive guide for Mesoporous Materials. Mesoporous materials are found abundant in biological systems and minerals and some of these materials have long been used in various industries. Recent advances at the nanoscale level has caused an increase in the use of these materials. This volume mainly discusses the analysis and functionalization of mesoporous materials.

Contents:

COMPREHENSIVE GUIDE FOR MESOPOROUS MATERIALS, VOLUME 2: ANALYSIS AND FUNCTIONALIZATION; COMPREHENSIVE GUIDE FOR MESOPOROUS MATERIALS, VOLUME 2: ANALYSIS AND FUNCTIONALIZATION; Library of Congress Cataloging-in-Publication Data; Contents; Preface; Chapter 1: Mesoporous Surface Structure Analysis; Abstract; 1. Introduction; 2. Definitions; 3. Measuring methods; Tracing; Grain Size Analysis; Optical Methods; Density Determination; Intrusion Porometry; Gas Adsorption; Adsorption from Solution; Size Exclusion; Calorimetry; Standardisation and Classification; References

Chapter 2: Twenty Years of Functionalized Mesoporous SilicaAbstract; Introduction; Functionalization of the Channel Pores; Functionalization of the Framework; The Multi-Functionalization; Multi-Functionalization in the Pores; Multi-Functionalization Pores-Walls; Conclusion; References; Chapter 3: Mesoporous Nanospheres of Titania Directly Modified with Tungstosilicic Acid As Catalysts in the Photodegradation of 4-Chlorophenol; Abstract; 1. Introduction; 2. Principles, Preparation and Characterization; 3. Results and Discussion; Conclusion; Acknowledgments; References

Chapter 4: Dual, Amorphous and Crystalline Characteristics in Pore Walls of Mesoporous FerrisilicatesAbstract; Introduction; Syntheses; Syntheses of Samples Used in the Present Study; Methods for Structural Characterisation of Mesoporous Ferrisilicates; Methods Applied for Characterisation of the Presented OS and SS Samples; X-Ray Diffraction; Specific Surface Area, Pore Size Distribution and Wall Thickness; TEM Measurements; Infrared Spectroscopy Combined with Pyridine Sorption; Temperature Programmed Reduction (TPR); Mössbauer Spectroscopy; Results of Characterisation of Applied Samples

X-Ray DiffractionSurface Area and Pore Size-Distribution; Transmission Electron Microscopy - Morphology; FTIR - Pyridine Sorption; Temperature Programmed Reduction (TPR); Mössbauer Spectroscopy; Discussion; Mesoporous Structure - General Scope; Local Structure around Embedded Iron; Flexibility of Environments Reflected in Fe3+ ( Fe2+ Redox Processes; Comparison of Behaviour of Iron Embedded into Mesoporous and into Microporous Ferrisilicates; Variations in the Extent of Crystallinity - Comparison of SS and OS Samples; Conclusion; Acknowledgment; References

Chapter 5: Functionalization of Mesoporous MaterialsAbstract; 1. Introduction; 2. Functionalization of Mesoporous Materials; 2.1. Generation of More Existing Groups; 2.2. Introduction of Other Functional Groups in the Mesoporous Materials; 2.2.1. Introduction of Heteroatoms; 2.2.2. Introduction of Nanoparticles; 2.2.3. Incorporation of Electroactive Substances in OMC; 2.3. Functionalization of Mesoporous Materials for the Construction of Electrochemical Biosensors; 2.3.1. Immobilization of Biomolecules on Mesoporous Materials with Usual Pore Size

2.3.2. Incorporation of Active Molecules in OMC with Large Pore

Notes:

Description based upon print version of record.

Includes bibliographical references and index.

Description based on online resource; title from PDF title page (ebrary, viewed May 15, 2015).

ISBN:

1-63463-991-X