Handbook of high field dynamic nuclear polarization / editors, Vladimir K. Michaelis.

Format:

Book

Contributor:

Michaelis, Vladimir K., editor.

Series:

eMagRes books.

eMagRes books

Language:

English

Subjects (All):

Polarization (Nuclear physics).

Physical Description:

1 online resource (478 pages).

Place of Publication:

West Sussex, England : Wiley, [2020]

Summary:

Addresses Dynamic Nuclear Polarization (DNP) as a technique for sensitivity-enhancement in solid-state NMR spectroscopy This comprehensive handbook is a compendium of the current state-of-the art of high field Dynamic Nuclear Polarization-from long-proven, early developments, up to today's hot topics. It covers all the relevant subjects that have made a direct or indirect contribution toward advancing this field, and focuses on topics such as: the theory behind the effects seen within DNP; instrumentation required for carrying out DNP; and specific applications of DNP including protein monitoring, catalysis, nanoparticles, biological and clinical studies. Development and application of techniques that have indirectly contributed to advancing MAS DNP NMR, such as DNP experiments on static solids within microwave resonant structures, and high-field EPR, are also examined. Handbook of High Field Dynamic Nuclear Polarization is presented in three sections-Theoretical Aspects, DNP Development (instrumentation / radical / sample), and DNP NMR Applications. The first section offers chapters on; solid and cross effect DNP; thermal mixing; Overhauser; and dissolution DNP. The second looks at: microwave technology, gyrotron, and IOE; homebuilt and commercial DNP spectrometers; and glassing vs. solvent-free DNP. The final section provides information on; amyloid, membrane, and nanocrystalline proteins; metals, and surface enhanced DNP; pharmaceuticals; nanoparticles; and much more. * Covers one of the biggest developing fields in magnetic resonance * Relevant to students, academics, and industry within the physical, materials, medical, and biochemical sciences * An excellent starting point and point-of-reference for researchers in the field * Edited by a widely respected team with contributions from key researchers in the NMR community * Part of the eMagRes Handbook Series Handbook of High Field Dynamic Nuclear Polarization is an ideal reference for all researchers and graduate students involved in this complex, interdisciplinary field. About eMagRes Handbooks eMagRes publishes a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence of this large number of articles, written by experts in various fields, is enabling the publication of a series of eMagRes Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of eMagRes articles. In consultation with the eMagRes Editorial Board, the eMagRes Handbooks are coherently planned in advance by specially-selected Editors, and new articles are written to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry. Have the content of this Handbook and the complete content of eMagRes at your fingertips! Visit: www.wileyonlinelibrary.com/ref/eMagRes

Contents:

The discovery and demonstration of dynamic nuclear polarization

a personal and historical account / Charles P. Slichter

DNP mechanisms / Krishnendu Kundu, Frédéric Mentink-Vigier, Akiva Feintuch, and Shimon Vega

Pulsed dynamic nuclear polarization / Kong Ooi Tan, Sudheer Jawla, Richard J. Temkin, and Robert G. Griffin

MAS-DNP enhancements : hyperpolarization, depolarization, and absolute sensitivity / Sabine Hediger, Daniel Lee, Frédéric Mentink-Vigier, and Gaël De Paëpe

Polarizing agents : evolution and outlook in free radical development for DNP / Gilles Casano, Hakim Karoui, and Olivier Ouari

Paramagnetic metal ions for dynamic nuclear polarization / Björn Corzilius

Instrumentation for high-field dynamic nuclear polarization NMR spectroscopy / Guy M. Bernard and Vladimir K. Michaelis

Millimeter-wave sources for DNP-NMR / Monica Blank and Kevin L. Felch

Cryogenic platforms and optimized DNP sensitivity / Yoh Matsuki and Toshimichi Fujiwara

Versatile dynamic nuclear polarization hardware with integrated electron paramagnetic resonance capabilities / Alisa Leavesley, Ilia Kaminker, and Songi Han

Dissolution dynamic nuclear polarization methodology and instrumentation / Dennis Kurzbach and Sami Jannin

Introduction to dissolution DNP : overview, instrumentation, and human applications / Jan H. Ardenkjaer-Larsen

Liquid-state Overhauser DNP at high magnetic fields / Vasyl P. Denysenkov and Thomas F. Prisner

Overhauser DNP in liquids on 13C nuclei / Marina Bennati and Tomas Orlando

DNP and cellular solid-state NMR / Alessandra Lucini Paioni, Marie A.M. Renault, and Marc Baldus

Cryo-trapped intermediates of retinal proteins studied by DNP-enhanced MAS NMR spectroscopy / Johanna Becker-Baldus and Clemens Glaubitz

DNP solid-state NMR of biological membranes / Burkhard Bechinger

DNP in materials science : touching the surface / Pierrick Berruyer, Lyndon Emsley, and Anne Lesage

Growing signals from the noise : challenging nuclei in materials DNP / Frédéric A. Perras, Takeshi Kobayashi, and Marek Pruski

DNP-enhanced solid-state NMR spectroscopy of active pharmaceutical ingredients / Li Zhao, Arthur C. Pinon, Lyndon Emsley, and Aaron J. Rossini

In vivo hyperpolarized 13C MRS and MRI applications / Irene Marco-Rius and Arnaud Comment

Dissolution dynamic nuclear polarization / Walter Köckenberger.

Notes:

Description based on print version record.

ISBN:

9781119441663

1119441668

9781119441694

1119441692