Fourier transform infrared spectroscopy : developments, techniques and applications / Oliver J. Rees, [editor].

Format:

Book

Contributor:

Rees, Oliver J.

Series:

Chemical engineering methods and technology.

Chemical engineering methods and technology

Language:

English

Subjects (All):

Fourier transform infrared spectroscopy.

Physical Description:

1 online resource (229 p.)

Edition:

1st ed.

Place of Publication:

New York : Nova Science Publishers, c2010.

Language Note:

English

Summary:

Fourier Transform Infrared Spectroscopy (FTIR) is a powerful tool for identifying types of chemical bonds in a molecule by producing an infrared absorption spectrum that is like a molecular 'fingerprint'. This book presents topical research in the field of FTIR including an overview of applications of FTIR spectroscopy.

Contents:

Intro

FOURIER TRANSFORM INFRARED SPECTROSCOPY: DEVELOPMENTS, TECHNIQUES AND APPLICATIONS

CONTENTS

PREFACE

FOURIER TRANSFORM INFRARED (FTIR) SPECTROSCOPY: DEVELOPMENT, TECHNIQUES, AND APPLICATION IN THE ANALYSES OF FATS AND OILS

ABSTRACT

INTRODUCTION

INFRARED (IR) SPECTROSCOPY

Infrared Absorption Process

Instrumentation

IR Spectra of Fats and Oils

Sample Handling Technique

1. Transmission Technique

2. Attenuated Total Reflectance (ATR)

Chemometric Data Analysis

APPLICATION OF FTIR SPECTROSCOPY IN FATS AND OILS ANALYSES

Analysis of Various Quality Parameters of Fats and Oils

1. Iodine value and Saponification Value

2. Free Fatty Acid

3. Peroxide Value (PV)

4. Anisidine Value and Aldehydes

5. Thiobarbituric Acid Reactive Substances

6. Isolated Trans Content

7. Moisture Content

8. Slip Melting Point and Cloud Point

9. Solid Fat Index

Analysis of Minor Components and Contaminants in Fats and Oils

Authentication of Fats and Oils

Monitoring Oxidation of Vegetable Oils

ACKNOWLEDGMENTS

REFERENCES

A MODIFIED FOURIER SERIES METHOD FOR THE DYNAMIC ANALYSIS OF STRUCTURES

A MODIFIED FOURIER SERIES METHOD FOR SOLVING BOUNDARY VALUE PROBLEMS

VIBRATIONS OF BEAMS WITH GENERAL BOUNDARY CONDITIONS

VIBRATIONS OF TWO ARBITRARILY COUPLED BEAMS

VIBRATIONS OF MULTI-SPAN BEAMS

EXTENDING THE MODIFIED FOURIER SERIES METHOD TO 2-D STRUCTURAL COMPONENTS - PLATES WITH ARBITRARY BOUNDARY CONDITIONS

DYNAMIC ANALYSIS OF COMPLEX STRUCTURES

CONCLUSION

APPENDIX A: EXPRESSIONS OF H, Q, S AND Z MATRICES

REFERENCES.

FIBER OPTIC-COUPLED GRAZING ANGLE PROBE-FOURIER TRANSFORM REFLECTION ABSORPTION INFRARED SPECTROSCOPY FOR ANALYSIS OF ENERGETIC MATERIALS ON SURFACES

SAMPLES AND STANDARDS PREPARATION

INSTRUMENTAL SETUP AND SPECTROSCOPIC PARAMETERS

SOLVENT SELECTION FOR SURFACE DEPOSITING

FOC-RAIRS OF NITRO AND NON-NITRO ENERGETIC MATERIALS ON METALLIC SURFACES

FOC-GAP-RAIRS SPECTRA OF 2,4,6-TNT DEPOSITED ON NON TRADITIONAL SURFACES

CHEMOMETRICS MODELS AND DISCRIMINANT ANALYSIS

APPLICATION OF CHEMOMETRIC MODELED FOURIER TRANSFORM INFRARED SPECTROMETRIC DATA FOR DIAGNOSTIC INVESTIGATION OF CANCER VIA TISSUE AND BLOOD ANALYSIS

VIBRATIONAL SPECTROSCOPIC FEATURES OF CELL BIOCHEMICALS

THEORETICAL DESCRIPTION OF APPLIED CHEMOMETRIC TECHNIQUES

ANALYSIS OF COLON CANCER TISSUE SAMPLES

Samples, Instruments and Software

Comparison of Spectral Data for Colon Cancer Tissue Samples

RESULTS AND DISCUSSIONS

ANOVA and PCA Results

LDA Results

SIMCA Results

ANALYSIS OF BLOOD SAMPLES FOR CANCER DETECTION

Spectrometric Findings

Results and Discussion

LDA Results for General Discrimination

SIMCA Results for BCC Diagnosis

CONCLUDING REMARKS

SIMULATOR PHOTOREACTOR FOR THE CHEMICAL CHARACTERIZATION OF DIESEL EXHAUST EMISSIONS

CHEMICAL TRANSFORMATIONS OF DIESEL EXHAUST EMISSIONS

A) Primary Diesel Emissions

B) Atmospheric Transformations of Diesel Exhaust Emissions

MONITORING OF DIESEL EXHAUST EMISSIONS

SMOG CHAMBER FOR DIESEL EXHAUST MONITORING

A) Instrumentation

B) Smog Chamber Experiment for Exhaust Monitoring

C) Limitations of Smog Chambers

DIESEL EXHAUST STUDIES IN SMOG CHAMBERS

CASE STUDY: MONITORING OF PAHS.

CONCLUSION

1. INTRODUCTION

2. UNIVERSAL ATTENUATED TOTAL REFLECTANCE FOURIER TRANSFORM SPECTROSCOPY

2.1. FTIR Study of Cotton Fiber Development

2.2. FTIR Study of Cotton Fiber Contamination

2.3. UATR-FTIR Study of Chemical Cross-Linking of Cotton Fabric

FTIR Integrated Intensity vs. %DMUG

3. FTIR IMAGING

EVALUATION OF SAMPLES AND STANDARDS OF ENERGETIC MATERIALS ON SURFACES BY GRAZING ANGLE-FTIR SPECTROSCOPY

RESIDENCE TIME AND SUBLIMATION KINETICS

HOMOGENEITY OF DISTRIBUTIONS ON SS SURFACES

METASTABLE PHASES OF TNT AND RDX

AN IN SITU FTIR FIBER OPTIC METHOD FOR THE DETECTION OF ACTIVE PHARMACEUTICAL INGREDIENTS AND EXCIPIENTS ON METALLIC SUBSTRATES

BACKGROUND AND RATIONALE

SAMPLE PREPARATION

IN SITU FTIR-BASED SCREENING TECHNIQUE

QUALITATIVE ANALYSIS OF SPECTRA

DEVELOPMENT OF A CALIBRATION MODEL

DISCRIMINANT ANALYSIS (DA)

STRUCTURAL MODIFICATION OF SINGLE WALL CARBON NANOTUBES BY GAMMA IRRADIATION

2. EXPERIMENTAL PROCEDURE

3. RESULTS AND DISCUSSION

3.1.Raman Spectroscopy

3.2. FTIR Spectroscopy

3.3. Atomic Force Microscopy

3.4. Stabilization Mechanism of Nanotube Dispersions

INDEX.

Notes:

Description based upon print version of record.

Includes bibliographical references and index.

ISBN:

1-61324-383-9

OCLC:

733057998