Materials syntheses : a practical guide / Ulrich Schubert, Nicola Husing, Richard Laine (eds.).

Format:

Book

Contributor:

Schubert, U. (Ulrich)

Hüsing, Nicola.

Laine, Richard M., 1947-

Language:

English

Subjects (All):

Organic compounds--Synthesis.

Organic compounds.

Chemistry, Organic.

Physical Description:

1 online resource (233 p.)

Edition:

1st ed. 2008.

Place of Publication:

Wien ; New York : Springer, c2008.

Language Note:

English

Summary:

Materials syntheses are generally more complex than syntheses of inorganic or organic compounds, and specific characterization methods play a more important role. Materials synthesis protocols often suffer from unclarities, irreproducibility, lack in detail and lack in standards. The need to change this situation is the main motivation for this book. A number of detailed protocols has been collected, ranging from organic polymers to carbonaceous and ceramic materials, from gels to porous and layered materials and from powders and nanoparticles to films. Preparation methods include intercalation and flux methods, sol-gel processing, templating methods for porous materials, sonochemistry or spray pyrolysis. Each contribution provides detailed and unambiguous description of the hardware, specific characteristics of the procedure, scope of applicability as well as methods that unequivocally identify and characterize the material and allow checking whether the synthesis was successful.

Contents:

Controlling Size and Morphology of Zeolite L

Zeolite A and ZK-4

Mesostructured Silica Thin Films

Organically Modified Monolithic Silica Aerogels

Porous Silica Gel by Acid Leaching of Metakaolin

Zirconia-Pillared Clays

Montmorillonites with Mixed Aluminum-Lanthanide Oxide Pillars

Birnessite-type Manganese Oxide by Redox Precipitation

Templated Carbon from Pyrolysis of Pyrene in Pillared Clay Matrices

Fiberous Carbon from Sepiolite Clay and Propylene

Aerosol Spray Synthesis of Porous Molybdenum Sulfide Powder

Sonochemically Prepared Molybdenum Sulfide

Doped Manganites

Lithium Manganese Oxide Prepared by Flux Methods

Nanoscale Magnesium Oxide

Nanostructured Pt-doped Tin Oxide Films

Organically Functionalized Silica Nanoparticles

Copper Nanoparticles in Silica

Copper Nanocrystals

Assembly of TOPO-Capped Silver Nanoparticles to Multilayered Films

Colloidal Dispersion of Gold Nanoparticles

One-dimensional Nanorods and Nanowires

Monolithic Tin-doped Silica Glass

Octaphenyloctasilsesquioxane and Polyphenylsilsesquioxane for Nanocomposites

Polysilsesquicarbodiimide Xerogels

Polyaniline — A Conducting Polymer

Allyl- and Hydroxytelechelic Poly(isobutylenes)

Symmetrically and Unsymmetrically Substituted Phthalocyanines.

Notes:

Description based upon print version of record.

Includes bibliographical references and index.

ISBN:

1-281-91373-1

9786611913731

3-211-75125-4

OCLC:

311507579